From Table 1 and Figure 1, dry WTS proved to have high Al and Fe content and was therefore used for the leaching process. 98% analytical grade sulphuric acid (H2SO4) supplied by Rochelle Chemicals was diluted with distilled water to produce the desired normalities (1.0, 2.0, 2.5 and 3.0 N). Solid loading was varied from 3 g WTS/100 mL of leaching agent, 5 g WTS/100 mL of leaching agent to 10 g WTS/100 mL of leaching agent.
Elemental oxides compositions for wet and dry WTS
Sample type . | Na2O (%) . | K2O (%) . | MgO (%) . | CaO (%) . | TiO2 (%) . | MnO (%) . | Fe2O3 (%) . | Al2O3 (%) . | SiO2 (%) . | P2O5 (%) . |
---|---|---|---|---|---|---|---|---|---|---|
Dry WTS | 0.153 | 0.817 | 0.743 | 0.849 | 0.460 | 1.06 | 5.28 | 20.3 | 31.9 | 0.439 |
Wet WTS | 0.171 | 0.604 | 0.592 | 1.69 | 0.338 | 1.34 | 3.65 | 16.5 | 31.3 | 0.503 |
Sample type . | Na2O (%) . | K2O (%) . | MgO (%) . | CaO (%) . | TiO2 (%) . | MnO (%) . | Fe2O3 (%) . | Al2O3 (%) . | SiO2 (%) . | P2O5 (%) . |
---|---|---|---|---|---|---|---|---|---|---|
Dry WTS | 0.153 | 0.817 | 0.743 | 0.849 | 0.460 | 1.06 | 5.28 | 20.3 | 31.9 | 0.439 |
Wet WTS | 0.171 | 0.604 | 0.592 | 1.69 | 0.338 | 1.34 | 3.65 | 16.5 | 31.3 | 0.503 |